A student is investigating the effect of temperature on the rate of enzyme activity using a colorimeter. Explain the precautions the student should take to ensure the results obtained are valid and reproducible.

OCR A-Level Biology A (H420) — 1.2 Practical skills assessed in the practical endorsement · Explain · 4 marks · View as Markdown

Written & reviewed by James Millett — Biology (Imperial College London), PGCE Science (University of Cambridge).

A student sets up an experiment to measure the rate of an enzyme-controlled reaction at five different temperatures (10°C, 20°C, 30°C, 40°C, 50°C). They use a colorimeter to measure the absorbance of a coloured product formed over time. The student carries out three repeats at each temperature.

Model answer (4 marks)

1. Keep the pH constant – use the same buffer for all trials so that only temperature changes.
2. Pre‑incubate the enzyme and the substrate separately at the set temperature for a few minutes before mixing, to avoid a temperature jump.
3. Calibrate the colourimeter with a blank/reference cuvette before each series of readings to obtain accurate absorbance values.
4. Perform three repeats at each temperature; this allows calculation of a mean rate and identification of any outliers, improving reproducibility.

Examiner tips

  • State a specific variable to control (e.g. pH).
  • Explain the purpose of pre‑incubation and calibration.
  • Link repeats to mean calculation and error detection.

Common mistakes

  • Ignoring the need to keep pH constant.
  • Failing to pre‑incubate or mix at the wrong temperature.

Mark scheme (4 marks)

  1. Control of a named variable other than temperature to ensure validity
  2. Pre-incubation of enzyme and substrate separately at the required temperature before mixing
  3. Calibration of the colorimeter with a blank/reference cuvette to ensure accurate absorbance readings
  4. Explanation of why repeats improve reproducibility, linked to identifying anomalous results or calculating a mean

Key terms in this question

colorimeter · valid · reproducible

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